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41.
Junyan Zhong Rachel L. SleighterElodie Salmon Georgina A. McKeePatrick G. Hatcher 《Organic Geochemistry》2011,42(8):903-916
Molecular level characterization of complex biopolymers in nature is a key element to understanding the composition of natural organic matter (NOM) and fossil organic matter formation, such as kerogen and coal. Characterization of such geopolymers is difficult due to their heterogeneity and insolubility in common aqueous or organic solvents. Here, a strategy for extracting a representative sample is presented using the combined techniques of nuclear magnetic resonance (NMR) and Fourier transform ion cyclotron resonance mass spectrometry (FTICR-MS) for chemical analysis and characterization of NOM. A variety of NOM samples (wood, kerogen, bitumen, whole sediments) are shown as examples for implementing the strategy, which include solvent extractions using pyridine. For most samples, the extracts are confirmed to be chemically representative of the insoluble solid, by comparing the liquids NMR spectrum of the extract to that of the whole, unfractionated NOM utilizing high resolution magic angle spinning (HRMAS) NMR. To assist in unambiguous peak assignment, a technique for post acquisition spectral denoising, using wavelet transformation (WT), is also employed on the 1D and 2D NMR spectra. The findings from the NMR data lay a foundation for the subsequent electrospray ionization FTICR-MS analysis of the pyridine extracts, since this instrument has the limitation of only analyzing liquid samples. The FTICR-MS analyses can, therefore, be used to molecularly represent the structural components of the NOM. Various compositional insights have been obtained on these samples, indicating the efficacy of the analytical techniques used. 相似文献
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In dam safety assessment, it is customary to focus on stability analysis, and the safety factor is regarded as an assessment
index that cannot correctly reflect the effect of multi-factors and variable uncertainty. The factors that induce dam breaks
are complex and uncertain; however, three primary ones can be identified: hydrological factors, seepage and bank slope instability.
In this paper, the risk probability and the dam break threshold value for each factor individually, as well as coupled factors,
are studied. The threshold value is acquired using the relationship formula between risk probability and dam type. The Dongwushi
reservoir located in the Hebei province of China is taken as a case study. The results show that the dam break threshold values
for hydrological factors, seepage and bank slope instability are 2.53, 2.02 and 2.69, respectively. The integrated dam break
threshold value for the coupled factors is 1.25, which indicates that the dam is under serious stress according to the established
risk assessment standard. The safety factor is calculated as 1.15 using the Bishop method, which indicates that the dam is
under serious stress. The results obtained by the proposed method are consistent with those of the Bishop method. Finally,
the proposed theory and method are introduced into a dam safety evaluation system (DSES) for convenient and efficient dam
safety management. 相似文献
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Coupling effect diagnoses of quasi-stationary mesoscale vortex in Guangxi rainstorm process of China
The mesoscale weather system which affected the Guangxi flash-flood-producing rainstorm of China in June 2008 is a quasi-stationary mesoscale vortex. Its genesis and development is closely related to the coupling effects of weather systems in different scales and different latitudes. On the one hand, the coupling of synoptic scale high- and low-level jets provides the environmental conditions for development of vortices and vertical circulations in the mesoscale vortex; On the other hand, the coupling of waves in mid-latitude westerlies and perturbations in low-latitude warm-moist flow under the influence of complex terrain makes the mesoscale vortex circulations strengthened. With the piecewise potential vorticity (PV) inversion method, PV anomalies in different regions are analyzed; also the vortex-vortex interactions and vortex-background flow interactions are diagnosed. Thus, the reasons why the mesoscale is quasi-stationary at first, while developing and deepening later are indicated. Under the condition of coupling effects, the vertical motions accompanied with the mesoscale vortex can be diagnosed with the PV-ω inversion system based on the analysis of quasi-balanced flow. 相似文献
49.
Study on the failure process of high concrete dams subjected to strong earthquakes is crucial to reasonable evaluation of their seismic safety. Numerical simulation in this aspect involves dynamic failure analysis of big bulk concrete dam subjected to cyclic loading. The Rock Failure Process Analysis (RFPA) proposed by C.A. Tang, with successful applications to failure modeling of rock and concrete specimens mainly subjected to static loading, is extended for this purpose. For using the proposed model, no knowledge on the cracking route needs to be known beforehand, and no remeshing is required. Simulation of the whole process of elastic deformation, initiation and propagation of microcracks, severe damage and ultimate failure of concrete dams in earthquakes with a unified model is enabled. The model is verified through a shaking table test of an arch dam. Finally a practical gravity dam is employed as a numerical example. Considering the uncertainty in ground motion input and concrete material, typical failure process and failure modes of gravity dam are presented. Several small cracks may occur due to tension particularly at dam neck, dam faces and dam heel, and a few of them evolve into dominant ones. Relatively smaller earthquake may cause damage to the dam neck while a bigger one may bring on cracks at lower parts of the dams. Cracking at the dam bottom may incline to a direction almost perpendicular to the downstream face after propagating horizontally for a certain distance when the shaking is strong enough. 相似文献
50.
Based on Fourier-Bessel series expansion of wave functions,an analytical solution to 2-D scattering ofincident plane SV waves by circular cylindrical canyons with variable depthto-width ratios is deduced in this paper. Unlike other analytical solutions,this paper uses the asymptotic behavior of the cylindrical function to directly define the undetermined coefficients of scattered waves,thus,avoiding solving linear equation systems and the related numerical computation problems under high-frequency incident waves,thereby broadening the applicable frequency range of analytical solutions. Through comparison with existing analytical solutions,the correctness of this solution is demonstrated. Finally, the incident plane SV wave scattering effect under circular cylindrical canyons in wider frequency bands is explored. 相似文献